Abstract:
We separated and purified five chemical constituents of dried ginger by Diaion HP-20, Sephadex LH-20, silica gel and semi-preparative high performance liquid chromatography. Five gingerols were identified by physicochemical properties and MS and NMR spectroscopy techniques:4-(2-butyl-6-methyl-4
H-pyran-4-yl)-2-methoxyphenol (
1), 4-(2-hexyl-6-methyl-4
H-pyran-4-yl)-2-methoxyphenol (
2), 1-(4-hydroxy-3-methoxyphenyl)tridecane-3,5-diol (
3),10-gingerdiol (
4) and 1-1-(4-hydroxy-3-methoxy phenyl)-3-oxodecan-5-ylpyrrolidin-2-one (
5a,
5b). Compounds
1-
3,
5a,
5b are new compounds.