牛惠莹, 方鸿斌, 司盈盈, 郑玉忠, 王彦志. 姜皮中三个新化合物的分离与鉴定J. 药学学报, 2025, 60(4): 1046-1051. DOI: 10.16438/j.0513-4870.2024-1012
引用本文: 牛惠莹, 方鸿斌, 司盈盈, 郑玉忠, 王彦志. 姜皮中三个新化合物的分离与鉴定J. 药学学报, 2025, 60(4): 1046-1051. DOI: 10.16438/j.0513-4870.2024-1012
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NIU Hui-ying, FANG Hong-bin, SI Ying-ying, ZHENG Yu-zhong, WANG Yan-zhi. Isolation and identification of three new compounds from Zingiber officinale (Ginger) peelJ. Acta Pharmaceutica Sinica, 2025, 60(4): 1046-1051. DOI: 10.16438/j.0513-4870.2024-1012
Citation: NIU Hui-ying, FANG Hong-bin, SI Ying-ying, ZHENG Yu-zhong, WANG Yan-zhi. Isolation and identification of three new compounds from Zingiber officinale (Ginger) peelJ. Acta Pharmaceutica Sinica, 2025, 60(4): 1046-1051. DOI: 10.16438/j.0513-4870.2024-1012
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姜皮中三个新化合物的分离与鉴定

Isolation and identification of three new compounds from Zingiber officinale (Ginger) peel

    摘要
  • 摘要: 运用MCI Gel CHP-20、Sephadex LH-20和ODS等柱色谱结合半制备高效液相色谱等方法, 从姜皮正丁醇部位中分离得到3个新化合物。结合1D-NMR、2D-NMR、HR-ESI-MS、圆二色谱(CD) 和计算CD (ECD) 等方法鉴定其结构分别为dendranthemoside C (1)、zingpyranoside E (2)、zingpyranoside F (3)。

     

    Abstract: Three new compounds were isolated from the n-butanol fraction of Zingiber officinale (Ginger) peel by MCI Gel CHP-20, Sephadex LH-20, ODS and semipreparative high performance liquid chromatography. Their structures were identified as dendranthemoside C (1), zingpyranoside E (2), zingpyranoside F (3) by 1D-NMR, 2D-NMR, HR-ESI-MS, circular dichroism (CD) and ECD calculation techniques.

     

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