张敏, 曹庸, 杜方麓, 欧阳文, 袁勇. 山莓中两个新二萜的分离与鉴定J. 药学学报, 2007, 42(11): 1155-1158.
引用本文: 张敏, 曹庸, 杜方麓, 欧阳文, 袁勇. 山莓中两个新二萜的分离与鉴定J. 药学学报, 2007, 42(11): 1155-1158.
ZHANG Min, CAO Yong, DU Fang-lu, OU-YANG Wen, YUAN Yong. Isolation and identification of two new diterpenoid from Rubus corchorifolius L.fJ. Acta Pharmaceutica Sinica, 2007, 42(11): 1155-1158.
Citation: ZHANG Min, CAO Yong, DU Fang-lu, OU-YANG Wen, YUAN Yong. Isolation and identification of two new diterpenoid from Rubus corchorifolius L.fJ. Acta Pharmaceutica Sinica, 2007, 42(11): 1155-1158.

山莓中两个新二萜的分离与鉴定

Isolation and identification of two new diterpenoid from Rubus corchorifolius L.f

  • 摘要: 为研究山莓(Rubus corchorifolius L.f)的化学成分,应用硅胶柱色谱进行分离纯化,根据化合物的理化性质和波谱数据鉴定结构。本文分离鉴定了2个贝壳杉烷二萜化合物,其结构分别为对映-贝壳杉烷-3α,16α,17,19-四醇(1),对映-2-羰基-16α-羟基-贝壳杉烷-17-β-D-葡糖苷(2)。化合物1、2均为新化合物。

     

    Abstract: To study the constituents of Rubus corchorifolius L.f, the constituents were separated by using various chromatographies and the structures were identified on the basis of chemical and spectral analysis. Two compounds were isolated from Rubus corchorifolius L.f. Their structures were identified as ent-kauran-3β,16β,17,19-tetrol (1), ent-2-carbonyl-16β-hydroxy-kauran-17-β-D-glucoside (2). Compounds 1 and 2 are new compounds.

     

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