毕跃峰, 郑晓珂, 冯卫生, 史社坡. 卷柏中化学成分的分离与结构鉴定J. 药学学报, 2004, 39(1): 41-45.
引用本文: 毕跃峰, 郑晓珂, 冯卫生, 史社坡. 卷柏中化学成分的分离与结构鉴定J. 药学学报, 2004, 39(1): 41-45.
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BI Yue-feng, ZHENG Xiao-ke, FENG Wei-sheng, SHI She-po. Isolation and structural identification of chemical constituents from Selaginella tamariscina (Beauv.) SpringJ. Acta Pharmaceutica Sinica, 2004, 39(1): 41-45.
Citation: BI Yue-feng, ZHENG Xiao-ke, FENG Wei-sheng, SHI She-po. Isolation and structural identification of chemical constituents from Selaginella tamariscina (Beauv.) SpringJ. Acta Pharmaceutica Sinica, 2004, 39(1): 41-45.
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卷柏中化学成分的分离与结构鉴定

Isolation and structural identification of chemical constituents from Selaginella tamariscina (Beauv.) Spring

    摘要
  • 摘要: 目的研究中药卷柏(Selaginella tamariscina (Beauv.) Spring)水提物中的化学成分。方法用Sephadex LH-20及硅胶等色谱技术进行分离纯化,根据理化性质、光谱数据进行结构鉴定。结果得到9个化合物,分别鉴定为(2r,3s)-二氢-2-(3′,5′-二甲氧基-4′-羟基苯基)-3-羟甲基-7-甲氧基-5-乙酰基苯骈呋喃(1),3-羟基-苯丙酸-(2′-甲氧基-4′-羧基苯酚)酯(卷柏酯A,2),丁香脂素(3),1-(4′-羟基-3′-甲氧基苯基)丙三醇(4),阿魏酸(5),咖啡酸(6),香荚兰酸(7),丁香酸(8),7-羟基香豆素(9)。结论化合物1,2为新化合物,其余化合物均为首次从卷柏属植物中分离得到。

     

    Abstract: AimTo study the chemical constituents of the water-extracts of Selaginella tamariscina (Beauv.) Spring. MethodsVarious chromatographic techniques were used to separate and purify the constituents. Their physico-chemical properties and spectral data were used to elucidate the structures. Results Nine compounds were isolated and identified as (2r,3s)-dihydro-2-(3′,5′-dimethoxy-4′-hydroxyphenyl)-7-methoxy-5-acetyl-benzofuran (1), 3-hydroxy-phenpropionic acid-(2′-methoxy-4′-carboxy-phenol) ester (tamariscina ester A, 2), sygringaresinol (3), 1-(4′-hydroxyl-3′-methoxyphenyl)glycerol (4), ferulic acid (5), caffeic acid (6), vanillic acid (7), syringic acid (8), and umbelliferone (9). ConclusionCompound 1 and 2 are new compounds, and the others were isolated from Selaginella for the first time.

     

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