汪時中. 乾燥氫氧化鋁凝膠的製備J. 药学学报, 1954, 2(1): 57-62.
引用本文: 汪時中. 乾燥氫氧化鋁凝膠的製備J. 药学学报, 1954, 2(1): 57-62.
Wang Shih-chung. THE PREPARATION OF DRIED ALUMINIUM HYDROXIDE GELJ. Acta Pharmaceutica Sinica, 1954, 2(1): 57-62.
Citation: Wang Shih-chung. THE PREPARATION OF DRIED ALUMINIUM HYDROXIDE GELJ. Acta Pharmaceutica Sinica, 1954, 2(1): 57-62.

乾燥氫氧化鋁凝膠的製備

THE PREPARATION OF DRIED ALUMINIUM HYDROXIDE GEL

  • 摘要: 1.以明礬液倒入碳酸钠溶液中,混合液之酸度须控制为pH6(±0.5)。2.所得膠体,先用普通水洗滌,继用0.4%碳酸氢钾溶液在抽氣漏斗上洗滌?チ蛩猁之手續须一次完成之,烘乾以後即不能重行处理,否则,制酸力急速下降。3.乾燥可控制在90—110℃(约6—10小时),大量烘乾时应注意湿空氣之排出。4.产品的制酸力一般为250—280毫/克,最高达315.9毫升/克;硫酸鹽之含量远低於药典规定;游离鹼亦远低於苏联药典之规定。

     

    Abstract: A method for preparing the high acid-consuming-capacity dried aluminium hydroxide powder by the use of alum and soda or other alkali substance as raw material is described. 1) The best results were obtained by using soda as raw material for preparing the alkali solution. 2) The alum solution was added to the alkali solution until pH 5.5-6.5 was reached. 3) The sulfate was removed almost completely by washing with potassium bicarbonate solution(0.4%) before drying. 4) The aluminium hydroxide gel can be dried completely under 100-105℃(ca. 6 hrs.) without influencing the antacid activity. 5) The highest acid-consuming-capacity of the dried powder of aluminium hydroxide gel(free from any free alkali) was determined to be 315.9 ml, i.e. one gram dried sample will neutralize 315.9ml 0.1N HCl.

     

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