Abstract: One new phenyl glycoside and two new chlorophenyl glycosides wereisolated from rhizomes of Curculigo orchioides (Chinese name :Xian Mao ,Hypoxidaceae).Based on HRMS, FABMS, ¹H -, ¹³C - NMR and other spectral data as well as chemicalevidence.the structures of curculigoside B, curculigine B and C were elucidated to be2-β- D- glucopyranosyloxy - 5 - hydroxybenzyl - 2 '- methoxy- 6'- hydroxybenzoate(I),24- dichloro - 3 - methyl - 5 - methoxy - phenol - O -β- D- apiofuranosyl (1 - 6 )-β - D - glucopyanoside (Ⅲ) and 2, 4,6 - trichloro - 3 - methyl - 5 - methoxyphenol -O - β - D - xylopyranosyl ( 1 - 6 ) -β - D - glucopyranoside (Ⅳ), respectively.