田晶, 肖志艳, 陈雅研, 赵玉英, 王祝举. 夏枯草皂苷A的结构鉴定J. 药学学报, 2000, 35(1): 29-31.
引用本文: 田晶, 肖志艳, 陈雅研, 赵玉英, 王祝举. 夏枯草皂苷A的结构鉴定J. 药学学报, 2000, 35(1): 29-31.
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Tian Jing, Xiao Zhiyan, Chen Yayan, Zhao Yuying , Wang Zhuju, . STRUCTURE IDENTIFICATION OF VULGARSAPONIN AJ. Acta Pharmaceutica Sinica, 2000, 35(1): 29-31.
Citation: Tian Jing, Xiao Zhiyan, Chen Yayan, Zhao Yuying , Wang Zhuju, . STRUCTURE IDENTIFICATION OF VULGARSAPONIN AJ. Acta Pharmaceutica Sinica, 2000, 35(1): 29-31.
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夏枯草皂苷A的结构鉴定

STRUCTURE IDENTIFICATION OF VULGARSAPONIN A

    摘要
  • 摘要: 目的：研究夏枯草(Prunella vulgaris L.)果穗中的化学成分。方法：用色谱法分离夏枯草的化学成分，并用化学及波谱法鉴定其结构。结果：从夏枯草中分离得到6个化合物，根据理化性质和波谱数据鉴定其结构分别为β-香树脂醇（1），α-波甾醇（2），豆甾醇（3），豆甾-7-烯-3β-醇（4），咖啡酸（5）和2α，3α，24-三羟基-齐墩果-12-烯-28-酸-28-β-D-吡喃葡糖酯苷（6）。并将其亲脂性部分甲基化后用气质联用方法进行分析，从中分离鉴定了8个脂肪酸类化合物。 结论：化合物6为新化合物，命名为夏枯草皂苷A，化合物2～5为首次从夏枯草获得。

     

    Abstract: AIM：To study the constituents of the spikes of Prunella vulgaris L. METHODS: The constituents were separated by using various chromatographies and the structures were identified on the basis of chemical and spectral analysis. RESULTS: Six compounds were isolated from the spikes of Prunella vulgaris L., their structures were identified as β-amyrin (1),　α-spinasterol (2), stigmasterol (3),　stigmast-7-en-3β-ol (4), caffeic acid (5) and 2α,3α-24-trihydroxy-olean-12-ene-28-oic acid-28-O-β-D-glucopyranosyl ester (6). In addition, eight fatty acids were isolated and identfied by GC-MS from the lipid fraction. CONCLUSION: Compound 6 was a new saponin and named as vulgarsaponin A. Compounds 2～4 were obtained for the first time from this plant.

     

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