徐, 慧, 周志华. 九里香中香豆精的反相高效液相色谱法测定J. 药学学报, 1994, 29(11): 851-855.
引用本文: 徐, 慧, 周志华. 九里香中香豆精的反相高效液相色谱法测定J. 药学学报, 1994, 29(11): 851-855.
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H Xu, ZH Zhou, . STUDIES ON SEPARATION AND DETERMINATION OF SIX COUMARINS IN MURJ5cAYA PANICULATA(L)JACK BY RP-HPLCJ. Acta Pharmaceutica Sinica, 1994, 29(11): 851-855.
Citation: H Xu, ZH Zhou, . STUDIES ON SEPARATION AND DETERMINATION OF SIX COUMARINS IN MURJ5cAYA PANICULATA(L)JACK BY RP-HPLCJ. Acta Pharmaceutica Sinica, 1994, 29(11): 851-855.
shu

九里香中香豆精的反相高效液相色谱法测定

STUDIES ON SEPARATION AND DETERMINATION OF SIX COUMARINS IN MURJ5cAYA PANICULATA(L)JACK BY RP-HPLC

    摘要
  • 摘要: 报道了九里香中6种香豆精——九里香乙素(murpanidin)，九里香丙素(murpanicin)，海南九里香内酯(hainanmurpanin)，murragatin，merazin hydrate，murralogin的反相高效液相色谱法测定。用Nuckosil—C18键合相柱、乙腈-水-甲醇(30:100:10)为流动相，异补骨脂素为内标，320 nm为检测波长。方法简便易行。

     

    Abstract: A reversed phase HPLC method for separation and determination of six coumarins(murragatin．merazin hydrate，murpanidin，murpanicin，murralogin，hainanmurpanin)in Murrayspaniculata(L)Jack was established．An ODS column(YWG-C18)and mobile phase methnol—water--acetonitrile (10:100:30)were employed．Isoporalen was used as internal standard．The determination wavelength was set at 320 nm．The method is simple，sensitive，reproducible and has been used for sample analysis．

     

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