ISOLATION AND IDENTIFICATION OF WUBANGZISIDE C FROM POLYGALA CAUDATA REHD ET WILS
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Abstract
By polyamide and silica gel chromatography, a new xanthone C-glycoside, wubangziside C(Ⅰ), was isolated from the n-butanolie fraction of the ethanolic extract of the bark and root bark of Polygala caudata Rehd et Wils.On the basis of chemical properties and spectroscopic (IR, UV, MS, 1H-and 13C-NMR) analysis, the structure of Wubangziside C(Ⅰ), C25H28O15, mp 232~4℃, αD22±79° (c, 1.01, 50%MeOH), waselucidated to be 1,3,7-trihydroxy xanthone-2,4-C-di-β-D-glucopyranoside.
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